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Organic Electronics
    Moisture Transport through Ultra-Low Permeation Barriers
    Chemistry and Orientation with NEXAFS Spectroscopy
Nanoimprint Lithography
  Pattern Transfer and Stability
Polymers for Next-Generation Lithography
  Dissolution Fundamentals
  Surface and Bulk Chemistry of Chemically Amplified Photoresists
  NIST-Industry Partnerships
Dimensional Metrology with Small Angle X-ray Scattering
  Sidewall Angle Metrology
  Dimensional Changes during Fabrication
Characterization of Porous Low-k Dielectric Thin Films
 
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Dimensional Metrology with Small Angle X-ray Scattering

 

Introduction

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  • Industry lacks capability to rapidly measure sub-50 nm structures with sub-nm precision. “Grand Challenge”
  • NIST developed alternative for critical dimension metrology with Small Angle X-ray Scattering (CD-SAXS)
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    Objective

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    To develop CD-SAXS methodology to quickly, quantitatively, and non-destructively measure critical dimensions and feature shape with sub-nanometer resolution on production scale test samples.
     

    NIST Role

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  • Develop capability of CD-SAXS to meet demands outlined in the ITRS Roadmap for metrology.
  • Develop protocols for measuring critical parameters in test patterns for sub-50 nm fabrication
  • Develop a laboratory scale device as a prototype
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    Highlights

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  • CD-SAXS shown to be viable technology
  • Sub-nm precision in periodicity and line width
  • Sample measured non-destructively on order of seconds
  • Design and purchase of lab-scale system
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    Customers and Impact

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    Industry Press and Recognition:
    EE Times, Semiconductor International, Micro Magazine

    “Small angle x-ray scattering for sub-100 nm pattern characterization”
    Applied Physics Letters 83, 4059 (2003)

     

    NIST Contributors

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    Wen-li Wu*
    Ronald Jones*
    Tengjiao Hu
    Christopher Soles
    Bryan Vogt
    Eric Lin
     

    Collaborators:

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    Diego Casa (Argonne)
    Arpan Mahorowala (IBM)
    Martha Sanchez (IBM)
    George Barclay (Shipley)
     
     
     
     
     
     
     
     
     
     
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    Electronics Materials Group
    Polymers Division
    Materials Science and Engineering Laboratory

     
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