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Small Angle Neutron Scattering Facility

 
The US's leading neutron scattering facility is maintained by the NIST Center for Neutron Research. Neutron scattering is used to probe molecular and microstructural features of polymers and other materials. Within the Facility there is an 8 m beam line that is particularly useful for studies of polymers.
 

Small Angle Neutron Scattering Instrument

 
The 8-meter SANS instrument is located at the end of neutron guide NG-1 where the guide cross section is 50 mm x 50 mm. This is a moderate resolution instrument suitable for examining structural features in materials from roughly 1 to 100 nm in size.

The beam from the guide passes through a liquid-nitrogen cooled filter consisting of 20 cm of polycrystalline beryllium and 15 cm of single-crystal bismuth to remove fast neutrons and core gamma rays, respectively, from the beam. Following the filter, a variable speed, helical vane, mechanical velocity selector is used to tune the mean wavelength from 5 to 20 A with a fixed wavelength resolution, delta lambda/lambda (FWHM) = 0.25. The beam is collimated along a 4.5 m evacuated pre-sample flight tube with either a pair of circular apertures at its entrance and exit or, for higher resolution measurements, a 7-beam, converging pinhole collimation system that can be inserted in the flight path.

The instrument has an evacuable sample chamber with a computer-controlled translation stage that accommodates multi-specimen sample changers with up to 5 sample positions. The sample chamber is removable, providing access to a 60 cm diameter rotatable sample table for large pieces of apparatus such as electromagnets and cryostats.

The post-sample evacuated flight path consists of three shielded cylindrical sections which are mounted on a frame that can be rotated about the sample position by about 15 to reach larger scattering angles. The section which houses the detector rolls along rails in the frame to allow the sample-to-detector distance to be changed from 3.6 m to 2.0 m. Built into the detector shield is an externally adjustable positioning device for locating a beam stop in front of the detector.

The detector is a 64 cm x 64 cm position-sensitive proportional counter that utilizes rise-time position encoding and has a spatial resolution of about 10 mm. Counts from the detector accumulate in histogramming memory and are periodically transferred to disk on the instrument's dedicated data acquisition computer as well as to a color monitor which displays a current image of the data being collected. The instrument is operated through a user-friendly menu-driven interface. Completed data sets can be reduced on-line and transferred electronically to a remote site, or to PC/Mac diskettes in ASCII format.

 

Contacts Information

E.J. Amis (Polymer Division)
(301) 975-6681
Email: Eric.Amis@nist.gov

Charles Glinka
(301) 975-6242
Email: cglinka@nist.gov

 
NIST Materials Science & Engineering Laboratory - Polymers Division
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Research Facilities
   
bullet Small Angle X-ray Scattering
   
bullet X-Ray Reflectivity
   
bullet Neutron Reflectivity
   
bullet Small Angle Neutron Scattering
   
bullet Macromolecular Mass Spectrometry
   
bullet Fiber-Matrix Interface Strength
   
bullet Combinatorial Methods
   
bullet Optical Coherence Tomography
   
bullet Extrusion Visualization
   
bullet Mercury Dilatometer
   
 
 
 
 
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