The US's leading neutron scattering
facility is maintained by the NIST
Center for Neutron Research. Neutron scattering is used to probe
molecular and microstructural features of polymers and other materials.
Within the Facility there is an 8 m beam line that is particularly
useful for studies of polymers.
Small Angle Neutron Scattering Instrument
The 8-meter SANS instrument is
located at the end of neutron guide NG-1 where the guide cross section
is 50 mm x 50 mm. This is a moderate resolution instrument suitable
for examining structural features in materials from roughly 1 to 100
nm in size.
The beam from the guide passes through a
liquid-nitrogen cooled filter consisting of
20 cm of polycrystalline beryllium and 15 cm of single-crystal bismuth
to remove
fast neutrons and core gamma rays, respectively, from the beam.
Following the
filter, a variable speed, helical vane, mechanical velocity selector
is used to tune the
mean wavelength from 5 to 20 A with a fixed wavelength resolution,
delta
lambda/lambda (FWHM) = 0.25. The beam is collimated along a 4.5
m evacuated
pre-sample flight tube with either a pair of circular apertures
at its entrance and exit
or, for higher resolution measurements, a 7-beam, converging pinhole
collimation
system that can be inserted in the flight path.
The instrument has an evacuable sample chamber
with a computer-controlled
translation stage that accommodates multi-specimen sample changers
with up to 5
sample positions. The sample chamber is removable, providing access
to a 60 cm
diameter rotatable sample table for large pieces of apparatus such
as electromagnets
and cryostats.
The post-sample evacuated flight path consists
of three shielded cylindrical
sections which are mounted on a frame that can be rotated about
the sample
position by about 15 to reach larger scattering angles. The section
which houses the
detector rolls along rails in the frame to allow the sample-to-detector
distance to be
changed from 3.6 m to 2.0 m. Built into the detector shield is an
externally
adjustable positioning device for locating a beam stop in front
of the detector.
The detector is a 64 cm x 64 cm position-sensitive
proportional counter that
utilizes rise-time position encoding and has a spatial resolution
of about 10 mm.
Counts from the detector accumulate in histogramming memory and
are
periodically transferred to disk on the instrument's dedicated data
acquisition
computer as well as to a color monitor which displays a current
image of the data
being collected. The instrument is operated through a user-friendly
menu-driven
interface. Completed data sets can be reduced on-line and transferred
electronically
to a remote site, or to PC/Mac diskettes in ASCII format.